1. Home
  2. Jurnal Kimia VALENSI Volume 7, No. 1, May 2021
  3. Purnomo

Synthesis and Characterization of Ag/TiO2 Nanoparticles using Mirabilis jalapa Plant Extract

Frida Octavia Purnomo, Sari Sekar Ningrum, Sadwika Najmi Kautsari

Abstract


Green synthesized nanomaterials have been widely developed because of their less toxicity, low energy process, environmentally friendly, effective, cheap, and pollution-free. Green synthesis of silver doped titanium dioxide nanoparticles (Ag/TiO2 NPs) was carried out using Mirabilis jalapa plant extract. The plant extract was used as a reducing agent. The functional groups, morphology, and crystalline structure of as-synthesized Ag/TiO2 NPs were investigated by FT-IR, FESEM, and XRD. Analysis by FESEM confirmed that the morphology of Ag/TiO2 NPs is spherical with an average size of ~ 400 nm. Crystallite size for the Ag/TiO2 NPs was calculated by the Scherrer formula dan the average size found to be in the range of 15.72 nm. The result of XRD analysis showing the fcc structure for metallic silver and TiO2 particles in the anatase and rutile phases.

Keywords


Green synthesis; nanoparticles Ag/TiO2; Mirabilis jalapa

References


Alsharaeh EH, Bora T, Soliman A, Ahmed F, Bharath G, Ghoniem MG, Abu-Salah KM, Dutta J. 2017. Sol-gel-assisted microwave-derived synthesis of anatase Ag/Tio2/Go nanohybrids toward efficient visible light phenol degradation. Catalysts. 7(5). https://doi.org/10.3390/catal7050133

Amaliyah S, Pangesti DP, Masruri M, Sabarudin A, Sumitro SB. 2020. Green synthesis and characterization of copper nanoparticles using Piper retrofractum Vahl extract as bioreductor and capping agent. Heliyon. 6(8). e04636. https://doi.org/10.1016/j.heliyon.2020.e04636

Atarod M, Nasrollahzadeh M, Sajadi SM. 2016. Journal of Colloid and Interface Science Euphorbia heterophylla leaf extract mediated green synthesis of Ag/TiO2 nanocomposite and investigation of its excellent catalytic activity for reduction of variety of dyes in water. JOURNAL OF COLLOID AND INTERFACE SCIENCE. 462: 272–279. https://doi.org/10.1016/j.jcis.2015.09.073

Fatimah I, Mutiara NAL. 2016. Biosythesis of silver nanoparticles using putri malu (mimosa pudica) leaves extract and microwave irradiation method. Molekul. 11(2): 288. https://doi.org/10.20884/1.jm.2016.11.2.221

Gopalakrishnan M, Sheenu A, Varghese B, Dharani J, Saranya S. 2019. A green approach for synthesis and characterization of silver nanoparticlesand their anti-microbial activity. Rasayan Journal of Chemistry. 12(3): 1072–1076. https://doi.org/10.31788/RJC.2019.1235136

Jegadeeswaran P, Rajiv P, Vanathi P, Rajeshwari S, Venckatesh R. 2016. A novel green technology: synthesis and characterization of Ag/TiO2 nanocomposites using Padina tetrastromatica (seaweed) extract. Materials Letters. 166: 137–139. https://doi.org/10.1016/j.matlet.2015.12.058

Liu N, Zhu Q, Zhang N, Zhang C, Kawazoe N, Chen G, Negishi N, Yang Y. 2019. Superior disinfection effect of Escherichia coli by hydrothermal synthesized TiO2-based composite photocatalyst under LED irradiation: Influence of environmental factors and disinfection mechanism. Environmental Pollution. 247: 847–856. https://doi.org/10.1016/j.envpol.2019.01.082

Oktaviana. 2018. (Mirabilis jalapa) sebagai ovisida nyamuk Aedes aegypti Aedes aegypti. 1–125. http://repository.radenintan.ac.id/4088/1/SKRIPSI LENGKAP OKTAFIANA.pdf

Purnomo FO, Surahman H, Ivandini TA, Naniwa S, Yoshida H, Gunlazuardi J. 2018. Bismuth vanadate (BiVO4) as counter electrode in the newly developed catalysis zone of modified cadmium sulfide (CdS) sensitized solar cell for hydrogen production. AIP Conference Proceedings, 2023. https://doi.org/10.1063/1.5064101

Rao TN, Riyazuddin, Babji P, Ahmad N, Khan RA, Hassan I, Shahzad SA, Husain FM. 2019. Green synthesis and structural classification of Acacia nilotica mediated-silver doped titanium oxide (Ag/TiO2) spherical nanoparticles: Assessment of its antimicrobial and anticancer activity. Saudi Journal of Biological Sciences. 26(7): 1385–1391. https://doi.org/10.1016/j.sjbs.2019.09.005

Sumbal, Nadeem A, Naz S, Ali JS, Mannan A, Zia M. 2019. Synthesis, characterization and biological activities of monometallic and bimetallic nanoparticles using Mirabilis jalapa leaf extract. Biotechnology Reports. 22. e00338. https://doi.org/10.1016/j.btre.2019.e00338

Yousaf H, Mehmood A, Ahmad KS, Raffi M. 2020. Green synthesis of silver nanoparticles and their applications as an alternative antibacterial and antioxidant agents. Materials Science and Engineering C. 112(October 2019). 110901. https://doi.org/10.1016/j.msec.2020.110901


Full Text: PDF

DOI: 10.15408/jkv.v7i1.18875

Refbacks

  • There are currently no refbacks.


Copyright (c) 2021 Frida Octavia Purnomo, Sari Sekar Ningrum, Sadwika Najmi Kautsari

Creative Commons License
This work is licensed under a Creative Commons Attribution-ShareAlike 4.0 International License.