Formulation and Antioxidant Evaluation of Clay Masks Containing Robusta Coffee Pulp Extract
DOI:
https://doi.org/10.15408/pbsj.v7i2.47124Keywords:
antioxidants, clay mask, coffee bean pulp, formulation, physical propertiesAbstract
The pulp of robusta coffee (Coffea canephora L.) is known to contain chlorogenic acid compounds that have potential as antioxidants. The content of this compound can be utilized as an active ingredient in cosmetics such as clay masks. The main component that affects the physical properties of a clay mask is the clay base. This study aims to develop a clay mask formulation from robusta coffee pulp extract with variations in the concentration of base combinations, namely bentonite and kaolin, and to observe their effects on the physical properties of the dosage form. The base concentration variations used were 20% (F1), 25% (F2), and 30% (F3) with a bentonite to kaolin ratio of 1:2. The evaluation of physical properties included organoleptic tests, homogeneity tests, pH tests, spreadability tests, adhesion tests, viscosity tests, and drying time measurements. The evaluation results showed that all clay masks were homogeneous with pH values ranging from 5.15 ± 0.04 to 5.29 ± 0.12, spreadability values of 4.60 ± 0.22 to 4.74 ± 0.37 cm, adhesion values of 0.82 ± 0.11 to 1.16 ± 0.15 seconds, and viscosity ranged from 5501 ± 670.22 to 7567.67 ± 220.30 mPa.s, and drying time ranged from 20.60 ± 0.39 to 25.34 ± 0.80 minutes. Results of the antioxidant activity test indicated that the clay mask made from robusta coffee pulp extract is a powerful antioxidant with IC50 values of 28.31 ± 4.72 to 30.45 ± 5.69 ppm. Variations in the concentration of the clay mask base significantly (p < 0.05) affected the viscosity and drying time of the dosage form. In summary, the clay mask formulations satisfied the essential physical criteria and showed promise for cosmetic application. F3 emerged as the leading formula, exhibiting the highest antioxidant capacity, evidenced by its lowest IC₅₀ value.
References
Amalia, A., Elfiyani, R., Chenia, A., 2021. Peningkatan Laju Difusi Alisin dalam Sistem Fitosom Ekstrak Bawang Putih. J. Ilmu Kefarmasian Indones. 19, 1–8. https://doi.org/10.35814/jifi.v19i1.842
Ardhany, S.D., Kusumawardhani, E., Suling, C.A., Dzuary, F.H., Novaryatiin, S., 2022. Clay Mask Papilak (Mussaenda frondosa L.) terhadap Bakteri Penyebab Acne Vulgaris. Lumbung Farm. J. Ilmu Kefarmasian 3, 110–117.
Bawekes, S.M., Yudistira, A., Rumondor, E.M., 2023. Uji Kualitatif Kandungan Senyawa Kimia Perasan Jeruk Nipis (Citrus aurantifolia Swingle). Pharmacon 12, 373–377. https://doi.org/10.35799/pha.12.2023.49269
Dipahayu, D., Lestari, K.A.P., 2021. Evaluasi Fisik Masker Anti Jerawat Dengan Ekstrak Etanol Daun Ubi Jalar Ungu (Ipomoea batatas (L.) Varietas Antin-3. J. Pharmasci (Journal Pharm. Sci. 6, 69–73. https://doi.org/10.53342/pharmasci.v6i2.219
Elfiyani, R., Nursal, F., Deviyolanda, R., Shifa, S., 2023. Pemanfaatan Ekstrak Kulit Putih Semangka dalam Sediaan Masker Clay. J. Sains Farm. Klin. 10, 218–225. https://doi.org/10.25077/jsfk.10.2.218-225.2023
Fauziah, F., Alvanny, N., Andalia, K., 2022. Formulasi dan Evaluasi Masker Clay Anti Jerawat dari Ekstrak Etanol Daun Pepaya (Carica Papaya L.). J. Ris. Kefarmasian Indones. 4, 306–320. https://doi.org/10.33759/jrki.v4i3.283
Febriani, Y., Sembiring, R., 2021. Formulation and Antioxidant Activity of Clay Mask of Ethanol Extract Tamarillo (Solanum betaceum Cav.). Indones. J. Pharm. Sci. Technol. Supp 1, 22–30. https://doi.org/10.24198/ijpst.v1i1.36432
Harahap, M.R., 2017. Identifikasi Daging Buah Kopi Robusta (Coffea robusta) Berasal Dari Provinsi Aceh. Elkawnie J. Islam. Sci. Technol. 3, 201–210. https://doi.org/10.22373/ekw.v3i2.2770
Indriastuti, D., Dewi, M.L., Priani, S.E., 2022. Literature Review Formulasi Sediaan Masker Clay Antioksidan. Bandung Conf. Ser. Pharm. 2, 1129–1135. https://doi.org/10.29313/bcsp.v2i2.4850
Jami’ah, S.R., Ifaya, M., Pusmarani, J., Nurhikma, E., 2018. Uji Aktivitas Antioksidan Ekstrak Metanol Kulit Pisang Raja (Musa Paradisiaca sapientum) dengan Metode DPPH (2,2-Difenil-1-Pikrilhidrazil). J. Mandala Pharmacon Indones. 4, 33–38. https://doi.org/10.35311/jmpi.v4i1.22
Kemenkes RI, 2017. Farmakope Herbal Indonesia Edisi 2. Kementrian Kesehatan Republik Indonesia.
Krismayadi, K., Halimatushadyah, E., Apriani, D., Cahyani, M.F., 2024. Standarisasi Mutu Simplisia dan Ekstrak Etanol Daun Kemangi (Ocimum x afriacanum Lour.). Pharm. Genius 03, 67–81. https://doi.org/10.56359/pharmgen.v3i2.333
Kumalasari, E., Wulandari, R.A., Aisyah, N., Febrianti, D.R., Niah, R., 2023. Formulasi Sediaan Masker Clay dari Ekstrak Daun Pidada Merah (Sonneratia caseolaris) sebagai Antioksidan. J. Insa. Farm. Indones. 6, 55–64. https://doi.org/10.36387/jifi.v6i1.1363
Nugrahaeni, F., Amalia, A., Rohmah, F., 2025. Formulation of Facial Clay Mask from Red Glutinous Rice (Oryza sativa L. var. glutinosa) Bran Extract. Trop. J. Nat. Prod. Res. 9, 1996–2001. https://doi.org/10.26538/tjnpr/v9i5.17
Nursal, F.K., Amalia, A., Nining, N., Putri, D.A., Larasati, K.D., 2024. Development of Coffee Fruit Skin (Coffea canephora) formula as Antioxidant peel-off Masks. J. Sains Farm. Klin. 11, 118–126. https://doi.org/10.25077/jsfk.11.2.118-126.2024
Saerang, M.F., Jaya Edy, H., Siampa, P., 2023. Formulasi Sediaan Krim dengan Ekstrak Etanol Daun Gedi Hijau (Abelmoschus manihot L.) terhadap Propionibacterium acnes. Pharmacon 12, 350–357. https://doi.org/10.35799/pha.12.2023.49075
Shahidi, F., Ambigaipalan, P., 2015. Phenolics and polyphenolics in foods, beverages and spices: Antioxidant activity and health effects - A review. J. Funct. Foods 18, 820–897. https://doi.org/10.1016/j.jff.2015.06.018
Shakeel, A., Kirichek, A., Chassagne, C., 2021. Applied Clay Science Rheology and yielding transitions in mixed kaolinite / bentonite suspensions. Appl. Clay Sci. 211, 106206. https://doi.org/10.1016/j.clay.2021.106206
Syamsidi, A., Syamsuddin, A.M., Sulastri, E., 2021. Formulation and Antioxidant Activity of Clay Mask of Tomato ( Solanum lycopersicum L .) Lycopene Extract with Variation of Concentration of Kaoline and Bentonite Bases ). J. Farm. Galen. (Galenika J. Pharmacy) 7, 77–90. https://doi.org/10.22487/j24428744.2021.v7.i1.15462
Tungadi, R., Thomas, N.A., Paneo, M.A., Monoarfa, R.P., 2024. Formulasi dan Evaluasi Sediaan Masker Lumpur Ekstrak Bunga Rosella (Hibiscus Sabdariffa L.) menggunakan Basis Bentonit dan Kaolin. Indones. J. Pharm. Educ. 4, 336–345. https://doi.org/10.37311/ijpe.v4i2.18040
Widyaningrum, N., Murrukmihadi, M., Ekawati, S.K., 2012. Pengaruh Konsentrasi Ekstrak Etanolik Daun Teh Hijau (Camellia sinesis L.) dalam Sediaan Krim terhadap Sifat Fisik dan Aktivitas Antibakteri. Sains Med. J. Kedokt. dan Kesehat. 4, 147–156. https://doi.org/10.30659/sainsmed.v4i2.371
Winahyu, D.A., Marcellia, S., Diatri, M.I., 2021. Uji Aktivitas Antioksidan Ekstrak Kulit Buah Kopi Robusta (Coffea canephora Pierre ex A.Foehner) dalam Sediaan Krim. J. Farm. Malahayati 4, 82–92. https://doi.org/10.33024/jfm.v4i1.4470
Wulan, W., Yudistira, A., Rotinsulu, H., 2019. Uji Aktivitas Antioksidan Dari Ekstrak Etanol Daun Mimosa pudica Linn. Menggunakan Metode DPPH. Pharmacon 8, 106–113. https://doi.org/10.35799/pha.8.2019.29243
Yasir, A.S., Ade, M.U., Hamid Al Fikri, A., 2023. Aktivitas Antioksidan dari Kulit Ari Biji Kopi Robusta (Coffea canephora) dalam Formulasi Sediaan Gel. J. Farmagazine X, 50–56. https://doi.org/10.47653/farm.v10i1.643
Zainal, T.H., Ulfa, M., Nisa, M., Pawarrangan, T.J., 2023. Formulasi Masker Clay Ekstrak Kulit Buah Pisang Muli (Musa acuminata L.). J. Penelit. Farm. Indones. 12, 7–12. https://doi.org/10.51887/jpfi.v12i1.1760
Zhang, X., Zhang, Z., Tao, H., He, X., Hsu, K., Wang, W., Fang, X., Steel, A., 2023. Comprehensive assessment of the efficacy and safety of a clay mask in oily and acne skin. Ski. Res. Technol. 29, 13513. https://doi.org/10.1111/srt.13513
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